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ICP-AES同时测定南极石中的22种元素
引用本文:吴冬梅,陈满荣,屈海云,王安宝,何品刚.ICP-AES同时测定南极石中的22种元素[J].光谱实验室,2006,23(6):1170-1173.
作者姓名:吴冬梅  陈满荣  屈海云  王安宝  何品刚
作者单位:1. 华东师范大学化学系,上海市,200062;中国科学院上海硅酸盐研究所,上海市,200050
2. 扬州大学环境科学与工程学院,江苏省扬州市,225009
3. 中国科学院上海硅酸盐研究所,上海市,200050
4. 华东师范大学化学系,上海市,200062
摘    要:电感耦合等离子体原子发射光谱法(ICP-AES)同时测定南极石中的铜、铁、锌、钙、镁、锰、钴等22种元素的含量.优化了消解样品用酸,选择了适合的元素分析线.各元素测定的相对标准偏差为0.13%-5.14%,加标回收率为95.43%-108.68%,方法简单、可靠,具有良好的准确度和精密度.

关 键 词:电感耦合等离子体-原子发射光谱法  南极石  22种元素
文章编号:1004-8138(2006)06-1170-04
收稿时间:2006-07-07
修稿时间:2006-08-02

Simultaneous Determination of 22 Elements in Antarctic Rock by ICP-AES
WU Dong-Mei,CHEN Man-Rong,QU Hai-Yun,WANG An-Bao,HE Pin-Gang.Simultaneous Determination of 22 Elements in Antarctic Rock by ICP-AES[J].Chinese Journal of Spectroscopy Laboratory,2006,23(6):1170-1173.
Authors:WU Dong-Mei  CHEN Man-Rong  QU Hai-Yun  WANG An-Bao  HE Pin-Gang
Institution:1.Department of Chemistry,East China Normal University,Shanghal 200062 ,P, R, China;2.Shanghai Institute of Ceramics, CAS, Shanghai 200050, P. R. China;3.School of Environmental Science and Technology , Yangzhou University , Yangzhou ,Jiangsu 225009, P. R. China
Abstract:The major and trace elements in Antarctic rocks were determined by ICP-AES. The conditions were optimized by choosing proper instrument conditions and detection wavelengths. The relative standard deviations are 0. 13%-5. 14% and the recoveries are 95.43%-108. 68%. The proposed method was applied to the analysis of Antarctic rocks with satisfactory results.
Keywords:ICP-AES  Antarctic Rock  22 Elements  
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