| 模拟移动床色谱法纯化白藜芦醇 |
| |
| 引用本文： | 张建超,高丽娟.模拟移动床色谱法纯化白藜芦醇[J].光谱实验室,2012,29(1):150-152. |
| |
| 作者姓名： | 张建超 高丽娟 |
| |
| 作者单位： | 1. 湖北中医药大学药学院 430065
2. 辽宁科技大学化工学院 114051 |
| |
| 摘 要： | 采用三带模拟移动床色谱法纯化虎杖白藜芦醇。实验结果表明:模拟移动床色谱纯化白藜芦醇的工艺参数为:流动相为V(甲醇):V(水):1:1;4根IDL=10mm×200mm ODS制备柱;柱连接方式1-2-1;洗脱带流量1.0mL/min,精制带流量1.5mL/min,吸附带流量1.6mL/min,进样流量0.1mL/min,切换时间19min。
|
| 关 键 词： | 虎杖 白藜芦醇 模拟移动床色谱 反相ODS填料 |
Purification of Resveratrol by Simulated Moving Bed Chromatography |
| |
| ZHANG Jian-Chao
,
GAO Li-Juan.Purification of Resveratrol by Simulated Moving Bed Chromatography[J].Chinese Journal of Spectroscopy Laboratory,2012,29(1):150-152. |
| |
| Authors: | ZHANG Jian-Chao GAO Li-Juan |
| |
| Institution: | a (School of Pharmaceutical Sciences,Hubei University of Chinese Medicine,Wuhan 430065,P.R.China) a(School of Chemical Engineering,University of Science and Technology of Liaoning,Anshan,Liaoning 114051,P.R.China) |
| |
| Abstract: | Purification of resveratrol from polygonum cuspidatum was accomplished with three zones simulated moving bed chromatography.The parameters of purification for resveratrol with simulated moving bed chromatographic were as follows:mobile phase of methanol-water(1:1,V/V), 4 columns(IDL= 10mm×200mm,ODS stationary phase),columns connection of 1-2-1,the refine zone flow of 1.5mL/min,the extraction zone flow of 1.0mL/min,the sorption zone flow of 1.6mL/min,the injection sample flow of 0.lmL/min and the switch time of 19min. |
| |
| Keywords: | Polygonum Cuspidatum Resveratrol Simulated Moving Bed Chromatography RP-ODS Padding |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
