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| 裂解-气相色谱-质谱联用技术研究厚朴浸膏的热裂解 | |
| 引用本文： | 潘聪,缪恩铭,师艳萍,耿永勤,李雪梅,陈业高,杨叶昆.裂解-气相色谱-质谱联用技术研究厚朴浸膏的热裂解[J].光谱实验室,2012,29(2):1210-1214. |
| 作者姓名： | 潘聪 缪恩铭 师艳萍 耿永勤 李雪梅 陈业高 杨叶昆 |
| 作者单位： | 1. 云南省烟草化学重点实验室云南烟草科学研究院,昆明市高新区科医路41号 650106;云南师范大学化学与化工学院,昆明市一二一大街2号 650500 2. 云南省烟草化学重点实验室云南烟草科学研究院,昆明市高新区科医路41号,650106 3. 红云红河烟草(集团)有限责任公司技术中心,昆明市北郊上庄,650202 4. 云南师范大学化学与化工学院,昆明市一二一大街2号,650500 |
| 基金项目： | 国家烟草专卖局资助项目(110200902060);云南中烟工业有限责任公司资助项目(2010JC05、2010RK03);云南省应用基础研究面上项目(2009CD153) |
| 摘 要： | 采用在线热裂解-气相色谱-质谱联用技术(Py-GC-M S),模拟卷烟燃吸状态,对厚朴浸膏的热裂解行为进行研究。结果表明:厚朴浸膏的热裂解产物中共鉴定出49种挥发性成分,含量较高的成分为厚朴酚(27.95%)、4-甲氧基和厚朴酚(21.88%)、和厚朴酚(15.46%)、石竹烯(0.69%)、氧化石竹烯(0.59%)、古巴烯(0.43%)等。厚朴酚、和厚朴酚为厚朴主要活性成分,具有抗氧化、抗抑郁、抗菌等活性。该结果为厚朴浸膏在卷烟中的应用提供理论依据。 |
| 关 键 词： | 厚朴 热裂解 气相色谱-质谱法 |
Pyrolysis of Magnolia officinalis Extract by Py-GC-MS |
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| PAN Cong , MIAO An-Ming , SHI Yan-Ping , GENG Yong-Qin , LI Xue-Mei , CHEN Ye-Gao , YANG Ye-Kun.Pyrolysis of Magnolia officinalis Extract by Py-GC-MS[J].Chinese Journal of Spectroscopy Laboratory,2012,29(2):1210-1214. | |
| Authors: | PAN Cong MIAO An-Ming SHI Yan-Ping GENG Yong-Qin LI Xue-Mei CHEN Ye-Gao YANG Ye-Kun |
| Institution: | aa(Key Laboratory of Tobacco Chemistry of Yunnan Province,Yunnan Academy of Tobacco Science,Kunming 650106,P.R.China)b(Faculty of Chemistry and Chemical Engineering,Yunnan Normal University,Kunming 650500,P.R.China)c[R&D Center of Hongyun Honghe Tobacco(Group) Co.Ltd.,Kunming 650202,P.R.China] |
| Abstract: | The pyrolytic behaviour of Magnolia officinalis extract was studied by online pyrolysis-gas chromatography-mass spectrometry(Py-GC-MS) under simulation of cigarette with burning and sucking condition.The results showed that 49 kind of volatile products of pyrolytic products of Magnolia officinalis extract were identified.The main compounds included magnolol(27.95%),4-methoxyhonokiol(21.88%),honokiol(15.46%),caryophyllene(0.69%),caryophyllene oxide(0.59%),copaene(0.43%) and so on.Magnolol and honokiol are the main active components of Magnolia officinalis,which have anti-oxidation,anti-depressant,and antibacterial activity as well.The results could supply theory basis for application of Magnolia officinalis extract in cigarette. |
| Keywords: | Magnolia officinalis Pyrolysis GC-MS |
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