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压痕塑性变形诱导非晶合金的晶化
引用本文:闫志杰,李金富,周尧和,仵彦卿.压痕塑性变形诱导非晶合金的晶化[J].物理学报,2007,56(2):999-1003.
作者姓名:闫志杰  李金富  周尧和  仵彦卿
作者单位:(1)上海交通大学环境科学与工程学院,上海 200030; (2)上海交通大学金属基复合材料国家重点实验室,材料学院,上海 200030; (3)上海交通大学金属基复合材料国家重点实验室,材料学院,上海 200030;太原科技大学材料科学与工程学院,太原 030024
基金项目:国家自然科学基金;中国博士后科学基金;山西省自然科学基金;山西省青年学术带头人项目;太原科技大学校科研和教改项目
摘    要:利用透射电镜研究了Zr65Al7.5Ni10Cu12.5Ag5非晶合金的Vickers压痕内微观结构的变化. 结果发现,压痕塑性变形诱导非晶合金发生了晶化,在压头棱角下面的区域内有尺寸大于1 μm的晶体析出. 选区电子衍射分析表明,该析出相是稳定的CuZr2或NiZr2四方晶体,而没有析出该非晶合金在加热过程中的初生相二十面体准晶相,说明非晶合金的机械稳定性与热稳定性是有区别的. 打压痕过程中的温度升高是可以忽略的,本工作进一步证实了塑性变形诱导非晶合金晶化的主要动力是粘性流动而非局部热效应. 关键词: 非晶合金 塑性变形 粘性流动 局部热效应

关 键 词:非晶合金  塑性变形  粘性流动  局部热效应
文章编号:1000-3290/2007/56(02)/0999-05
收稿时间:2006-05-17
修稿时间:2006-05-172006-07-24

Indentation-induced crystallization in a metallic glass
Yan Zhi-Jie,Li Jin-Fu,Zhou Yao-He,Wu Yan-Qing.Indentation-induced crystallization in a metallic glass[J].Acta Physica Sinica,2007,56(2):999-1003.
Authors:Yan Zhi-Jie  Li Jin-Fu  Zhou Yao-He  Wu Yan-Qing
Institution:Sate Key Laboratory of Metal Matrix Composites, School of Materials Science and Engineering, Shanghai Jiantong University, Shanghai 200030, China; School of Mawrials Science and Engineering, Taiyuan Uniuersity of Science and Technology, Taiyuan 030024, China;School of Enrironmental Science and Engineering, Shanghai yiaotong University, Shanghai 200030, China
Abstract:The microstructure change in the Vickers indent of the Zr65Al7.5Ni10Cu12.5Ag5 metallic glass at room temperature is investigated by transmission electron microscopy. It is found that the indentation-induced crystallization occurs namely underneath the indenter edges, where viscous flow is involved and crystals with the size larger than 1 μm appeav. The selected area electron diffraction shows that the crystalline phases are stable tetragonal CuZr2 or NiZr2, but not the icosahedral one that grows as metastable phase on heating. The local temperature rise during indentation can be ignored, which further suggests that the mechanically induced crystallization in a metallic glass is attributed to the viscous flow rather than the local heating effect.
Keywords:amorphous alloys  plastic deformation  viscous flow  local heating effect
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