| N-(α,β-双取代-4-氯桂皮酰基)-另丁胺类化合物的NMR及构型研究 |
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| 引用本文： | 陈素明,彭师奇,刘维勤.N-(α,β-双取代-4-氯桂皮酰基)-另丁胺类化合物的NMR及构型研究[J].波谱学杂志,1985,2(1):13-17. |
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| 作者姓名： | 陈素明 彭师奇 刘维勤 |
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| 作者单位： | 1. 中国科学院化学研究所;2. 北京医学院药学系 |
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| 摘 要： | 本文报道了N-(α,β-双取代-4-氯桂皮酰基-另丁胺类化合物的1H NMR及13C NMR的研究。通过比较该类化合物分子酰胺基中氢及碳的化学位移指定了各化合物的构型。采用NMR方法判定的构型为X光衍射结果所证实。
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| 收稿时间： | 1984-08-15 |
THE STUDY OF NMR ON THE N-(α,β-DISUBSTITUTED-4-CHLOROCINNAMYL)-SEC.-BUTYLAMINE DERIVATIVES |
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| Chen Sumeng,Peng Shiqi,Liu Weiqin.THE STUDY OF NMR ON THE N-(α,β-DISUBSTITUTED-4-CHLOROCINNAMYL)-SEC.-BUTYLAMINE DERIVATIVES[J].Chinese Journal of Magnetic Resonance,1985,2(1):13-17. |
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| Authors: | Chen Sumeng Peng Shiqi Liu Weiqin |
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| Institution: | 1. Institute of Chemistry, Academia Sinica, Beijng;2. Department of Pharmaceutical Sciences, Beijing Medical College |
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| Abstract: | In the present paper the 1H NMR and 13C NMR spectral data of N-(α,β disu-bstituted-4-chloro-cinnamyl) -sec. -butylamine compounds were reported Compared the chemical shifts of hydrogen and carbon in the amide groups ofthe compounds, the configurations of the compounds were assigned.The configurations assigned according to NMR were proved by the results of X-ray diffraction of the crystals of the compounds. |
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