| 固体高分辨DNP CP/MAS探头的研制及DNP实验技术的探讨 |
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| 引用本文： | 杨保联,胡红兵.固体高分辨DNP CP/MAS探头的研制及DNP实验技术的探讨[J].波谱学杂志,1996,13(2):183-190. |
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| 作者姓名： | 杨保联 胡红兵 |
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| 作者单位： | 中国科学院武汉物理研究所波谱与原子分子物理国家重点实验室, 武汉 430071 |
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| 基金项目： | 国家自然科学基金，第三世界科学院资助 |
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| 摘 要： | 介绍了自行研制的用于动态核极化实验的固体高分辨CP/MAS探头,给出了典型含自由基固体样品的DNP增强高分辨NMR谱.并对动态核极化实验中的技术问题进行了讨论,提出了相应的解决方法.
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| 关 键 词： | 动态核极化 固体高分辨 CP/MAS |
| 收稿时间： | 1995-04-26 |
DNP CP/MAS PROBE DESIGN AND DISCUSSION OF DNP EXPERIMENTAL TECHNIQUE |
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| Yang Baolian,Hu Hongbing, Zhou Jianwei, Li Liyun,Qiu Jianqing, Zeng Fanming,Hu Jianzhi, and Ye Chaohui.DNP CP/MAS PROBE DESIGN AND DISCUSSION OF DNP EXPERIMENTAL TECHNIQUE[J].Chinese Journal of Magnetic Resonance,1996,13(2):183-190. |
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| Authors: | Yang Baolian Hu Hongbing Zhou Jianwei Li Liyun Qiu Jianqing Zeng Fanming Hu Jianzhi and Ye Chaohui |
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| Institution: | State Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Institute of Physics, The Chinese Academy of Sciences, Wuhan 430071 |
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| Abstract: | A high resolution solid state DNP CP/MAS probe was designed.By using this probe,high resolution NMR spectra of solid state samples containing free radicals were obtained.Some typical results are shown in this paper. Technical problems in DNP NMR experiment are discussed and some methods are suggested to deal with these problems. |
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| Keywords: | DNP Solid state high resolution NMR CP/MAS |
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