| 阴山大戟中一个对映海松烷型二萜2D NMR全归属 |
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| 引用本文： | 张本印,王环,罗晓东,杜芝芝,沈建伟,张晓峰.阴山大戟中一个对映海松烷型二萜2D NMR全归属[J].波谱学杂志,2012,29(1):112-118. |
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| 作者姓名： | 张本印 王环 罗晓东 杜芝芝 沈建伟 张晓峰 |
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| 作者单位： | 中国科学院西北高原生物研究所,青海西宁810008;中国科学院研究生院,北京100049;中国科学院西北高原生物研究所,青海西宁,810008;中国科学院昆明植物研究所植物化学与西部植物资源持续利用国家重点实验室,云南昆明,650204 |
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| 基金项目： | The open project of State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences (P2008-KF05); the project of western doctorate foundation and the knowledge innovation project from the northwest institute of plateau biology, Chinese Academy of Sciences. |
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| 摘 要： | 从阴山大戟的根部首次分到一个已知的对映-海松烷型二萜，3α, 19-dihydroxyl-ent-pimara-9, 15-diene，通过二维波谱方法（1H-1H COSY, HMBC, HMQC, ROESY）确定了其结构，并且首次此化合物的H谱和C谱数据进行了全归属.
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| 关 键 词： | 大戟科 阴山大戟 对映-海松烷型二萜 2D NMR谱 |
| 收稿时间： | 2011-03-28 |
| 修稿时间： | 2011-04-20 |
2D NMR Assignments of an ent-Pimarane Diterpenoid from Euphorbia yinshanica |
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| ZHANG Ben-yin,WANG Huan,LUO Xiao-dong,DU zhi-zhi,SHEN Jian-wei,ZHANG Xiao-feng.2D NMR Assignments of an ent-Pimarane Diterpenoid from Euphorbia yinshanica[J].Chinese Journal of Magnetic Resonance,2012,29(1):112-118. |
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| Authors: | ZHANG Ben-yin WANG Huan LUO Xiao-dong DU zhi-zhi SHEN Jian-wei ZHANG Xiao-feng |
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| Institution: | 1. Northwest Institute of Plateau Biology, Chinese Academy of Sciences, Xining 810008, China; ;
2. State Key Laboratory of Phytochemistry and Plant Resources in West China, Kunming Institute of Botany, Chinese Academy of Sciences, Kunming 650204, China；;
3. Graduate University of the Chinese Academy of Sciences, Beijing 100049, China |
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| Abstract: | One known ent pimarane type diterpenoid, 3α, 19-dihydroxyl ent pimara- 9(11), 15-diene, has been isolated from the roots of Euphorbia yinshanica for the first time. Its structure has been confirmed by 2D spectral methods (1H-1H COSY, HMBC, HMQC, ROESY), and its NMR signals have been first completely assigned. |
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| Keywords: | Euphorbiaceae " target="_blank">Euphorbia yinshanicazz')" href="#"> Euphorbia yinshanica " target="_blank">-pimarane diterpenoidzz')" href="#"> ent-pimarane diterpenoid 2D NMR |
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