| 哌嗪雌酚酮的结构研究 |
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| 引用本文： | 韩海,张强,李章万,翁玲玲,郑虎.哌嗪雌酚酮的结构研究[J].波谱学杂志,2001,18(4):305-314. |
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| 作者姓名： | 韩海 张强 李章万 翁玲玲 郑虎 |
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| 作者单位： | 四川大学华西药学院, 成都 610041 |
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| 基金项目： | 国家自然科学基金重点资助项目 |
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| 摘 要： | 哌嗪雌酚酮是一种可望用于骨质疏松症的雌激素类防治药物. 文中采用IR、MS、NMR 等波谱技术，特别是1H-1H COSY、HMQC和HMBC谱等2D NMR技术, 确定了它的氢谱和碳谱的信号归属，对它的结构进行了确证.
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| 关 键 词： | 哌嗪雌酚酮 结构 解析 2D NMR |
| 文章编号： | 1000-4556(2001)04-0305-10 |
| 收稿时间： | 2001-06-30 |
| 修稿时间： | 2001年6月30日 |
Structural Study of Piperazinylethylestrone Ether |
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| HAN Hai,ZHANG Qiang,LI Zhang-wan ,WENG Ling-ling and ZHENG Hu.Structural Study of Piperazinylethylestrone Ether[J].Chinese Journal of Magnetic Resonance,2001,18(4):305-314. |
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| Authors: | HAN Hai ZHANG Qiang LI Zhang-wan WENG Ling-ling and ZHENG Hu |
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| Institution: | Department of Pharmacy, Sichuan University, Chengdu 610041 |
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| Abstract: | Piperazinylethylestrone ether is a new synthesized compound that can be used for the prevention and treatment of osteoporosis and other disease caused by osteoporosis. For further study on it, in this article, the structure of piperazinylethylestrone ether was established by using a series of spectral techniques (e.g. IR, MS, NMR) especially two-dimensional 1H- 1H COSY, HMQC and HMBC which can provide valuable information. This combination of these techniques is applicable for the assignment of highly overlapping signals and makes it possible to completely assign the 1H and 13C NMR spectra signals of piperazinylethylestrone ether. |
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| Keywords: | Piperazinylethylestrone ether Structure Analyze 2D NMR |
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