| 吴茱萸碱、吴茱萸次碱和去氢吴茱萸碱的碳氢NMR信号全指定 |
| |
| 引用本文： | 张虎,杨秀伟,崔育新.吴茱萸碱、吴茱萸次碱和去氢吴茱萸碱的碳氢NMR信号全指定[J].波谱学杂志,1999,16(6):563-568. |
| |
| 作者姓名： | 张虎 杨秀伟 崔育新 |
| |
| 作者单位： | 北京医科大学天然药物及仿生药物国家重点实验室, 北京 100083 |
| |
| 基金项目： | 国家“九五”科技攻关资助!96-901-01-39 |
| |
| 摘 要： | 应用1DNMR和梯度2DNMR反相技术(gCOSY,gNOESY,gHMQC,gHMBC)研究了从疏毛吴茱萸中分离得到的三个生物碱:吴茱萸碱、吴茱萸次碱和去氢吴茱萸碱的结构,并对其碳氢NMR信号进行了全归属.
|
| 关 键 词： | 疏毛吴茱萸 吴茱萸碱 吴茱萸次碱 去氢吴茱萸碱 梯度2DNMR |
| 收稿时间： | 1999-06-30 |
COMPLETE ASSIGNMENT OF 1H AND 13C NMR CHEMICAL SHIFTS OF EVODIAMINE, RUTAECARPINE AND DEHYDROEVODIAMINE |
| |
| ZHANG Hu,YANG Xiuwei,CHUI Yuxin.COMPLETE ASSIGNMENT OF 1H AND 13C NMR CHEMICAL SHIFTS OF EVODIAMINE, RUTAECARPINE AND DEHYDROEVODIAMINE[J].Chinese Journal of Magnetic Resonance,1999,16(6):563-568. |
| |
| Authors: | ZHANG Hu YANG Xiuwei CHUI Yuxin |
| |
| Institution: | Beijing Medical University, National Research Laboratory of Natural and Biochetic Drugs, Beijing 100083 |
| |
| Abstract: | Three alkaloids, Evodiamine, Rutaecarpine and Dehydroevodiamine, were isolated fromthe fruits of Evndia rutaecarpa (Juss) var. bodinaieri (Dode) Huang. In this paper, all ofthe iH and 13C NMR chemical shifts of these compounds were assigned through iD NMRand 2D NMR with Pulse Field Gradient (PFG) techniques (gCOSY, gNOESY, gHMQC andgHMBC). |
| |
| Keywords: | Endia rutaecarpa (Juss) Benth var bodinaieri Evodiamine Rutaecarpine Dehydroevodiamine 2D NMR with Pulse Field Gradient (PFG) |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
| 点击此处可从《波谱学杂志》浏览原始摘要信息 |
| 点击此处可从《波谱学杂志》下载免费的PDF全文 |
