| 土大黄苷的NMR研究 |
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| 引用本文： | 刘力军,王林,李鲁,缪振春,赵玉梅.土大黄苷的NMR研究[J].波谱学杂志,2008,25(3):349-354. |
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| 作者姓名： | 刘力军 王林 李鲁 缪振春 赵玉梅 |
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| 作者单位： | （1. 军事医学科学院 毒物药物研究所，北京 100850; 2. 军事医学科学院 放射医学研究所，北京 100850 ） |
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| 摘 要： | 土大黄苷，3-羟基-5-2-（3-羟基-4-甲氧苯基）乙烯基]苯-β-D-葡萄糖苷是从植物中提取分离的单体化合物，应用1D NOE 和2D NMR（1H-1H COSY、HMQC、HMBC）等技术相结合的方法对土大黄苷的1H和13C NMR信号进行了准确归属，并对文献中错误的碳氢数据做了纠正和讨论.
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| 关 键 词： | NMR 归属 1D NOE 土大黄苷 |
| 收稿时间： | 2007-8-20 |
| 修稿时间： | 2007-12-24 |
An NMR Study on Rhapontin |
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| LIU Li-jun,WANG Lin,LI Lu,MIAO Zhen-chun,ZHAO Yu-mei.An NMR Study on Rhapontin[J].Chinese Journal of Magnetic Resonance,2008,25(3):349-354. |
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| Authors: | LIU Li-jun WANG Lin LI Lu MIAO Zhen-chun ZHAO Yu-mei |
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| Institution: | (1. Institute of Pharmacology and Toxicology, Academy of Military Medical Sciences, Beijing 100850, China; 2. Institute of Radiation Medicine, Academy of Military Medical Sciences, Beijing 100850, China) |
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| Abstract: | Rhapontin, 3-hydroxy-5-(2-(3-hydroxyl-4-methoxyphenyl) ethenyl) phenyl-β-D- glucopyranoside, was a natural product isolated from the plant. Its structure was elucidated by combined use of 1D NOE and 2D NMR techniques including 1H-1H COSY, HMQC and HMBC. The 1H and 13C chemical shifts of the compound were completely assigned. Corrections were made for the incorrect previous assignment. |
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| Keywords: | NMR 1D NOE |
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