| 新鞣花酸衍生物的NMR归属 |
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| 引用本文： | 冀亚飞,张培成,于德泉.新鞣花酸衍生物的NMR归属[J].波谱学杂志,2007,24(2):133-140. |
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| 作者姓名： | 冀亚飞 张培成 于德泉 |
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| 作者单位： | 1.华东理工大学 制药工程系，上海 200237；2.中国医学科学院中国协和医科大学 药物研究所，北京 100050 |
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| 摘 要： | 从鞣花酸(1)合成二个新的多取代的联苯化合物3和4，利用HMQC，HMBC和一维NOE谱技术确定了它们的13C和1H NMR归属.
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| 关 键 词： | 核磁共振 HMQC HMBC 一维NOE谱 联苯化合物 二异丁基氢化铝 |
| 文章编号： | 1000-4556（2007）02-0133-08 |
| 收稿时间： | 2006-6-5 |
| 修稿时间： | 2006-06-052006-07-17 |
NMR Assignment of Two Ellagic Acid Derivatives |
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| JI Ya-fei,ZHANG Pei-cheng,YU De-quan.NMR Assignment of Two Ellagic Acid Derivatives[J].Chinese Journal of Magnetic Resonance,2007,24(2):133-140. |
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| Authors: | JI Ya-fei ZHANG Pei-cheng YU De-quan |
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| Institution: | 1.Department of Pharmacy Engineering, East China University of Science and Technology, Shanghai 200237, China; 2.Institute of Meteria Medica, Chinese Academy of Medical Sciences & Peking Union Medical College, Xiannongtan Street, Beijing 100050, China |
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| Abstract: | Two polysubstituted biphenyl compounds were synthesized from ellagic acid. Using NMR techniques including HMQC, HMBC and 1D NOE techniques, the 13C and 1H NMR chemical shifts of the two product compounds were assigned. |
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| Keywords: | NMR HMQC HMBC 1D NOE biphenyl compounds Bui2AlH |
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