| 橄榄苦甙的NMR数据解析 |
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| 引用本文： | 赵天增,尹卫平,张海艳,付经国,吴鸣建.橄榄苦甙的NMR数据解析[J].波谱学杂志,2002,19(1):57-61. |
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| 作者姓名： | 赵天增 尹卫平 张海艳 付经国 吴鸣建 |
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| 作者单位： | 1.河南省科学院化学研究所，郑州 450002; 2.洛阳工学院，洛阳 471039 |
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| 基金项目： | 河南省自然科学基金资助项目（994030500） |
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| 摘 要： | 对橄榄苦甙进行了1H和13C MNR检测, 通过DEPT和1H-1H COSY、HMQC、HMBC、NO ESY等2D NMR对其1H和13C NMR数据进行了全归属和较详细的解析, 并指出其NMR数据特征.
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| 关 键 词： | 橄榄苦甙 1H和13C NMR 2D NMR 小 叶丁香 |
| 文章编号： | 1000-4556(2002)01-057-05 |
| 收稿时间： | 2001-08-08 |
| 修稿时间： | 2001年8月8日 |
NMR STUDY ON OLEUROPEIN |
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| ZHAO Tianzeng,YIN Weiping,ZHANG Haiyan,FU Jingguo and WU Mingjian.NMR STUDY ON OLEUROPEIN[J].Chinese Journal of Magnetic Resonance,2002,19(1):57-61. |
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| Authors: | ZHAO Tianzeng YIN Weiping ZHANG Haiyan FU Jingguo and WU Mingjian |
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| Institution: | 1.Chemistry Institute, Henan Academy of Science, Zhengzhou 450002, China;
2.Luoyang Institute of Science and Techonolgy, Luoyang 471039, China |
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| Abstract: | Oleuropein is a well-known secoiridoid glucoside which is rich in the Oleaceae family. Its structure was confirmed during 1960～1974. It has been isolated from ma ny plants of the genus Olea, Fraxinus, Jasminum, Ligustrumand Syringato d ate. Its NMR data has been reported, but the detailed elucidation has not been given. Ou r recent study on the leaves of Syringa pubescens Turcz.(a Chinese folk her b)has resulted in the isolation o f this constituent for the first time. In this paper, by utilizing a combination of 1D and 2D NMR techniques, its 1H and 13C NMR spectra are completely assigned and detailedly analyzed and the characteristics of its NMR data are also pointe d out. |
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| Keywords: | oleuropein 1H and 13C NMR 2D NMR syringa pubescens turcz |
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