| 酞菁氧钛的合成及晶型转化 |
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| 引用本文： | 王竹庭,鲁开娟.酞菁氧钛的合成及晶型转化[J].应用化学,1994,11(1):72-75. |
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| 作者姓名： | 王竹庭 鲁开娟 |
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| 作者单位： | 中国科学院化学研究所 |
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| 摘 要： | 酞菁氧钛以联环己烷为溶剂，以邻苯二脂及四氯化钛直接反应生成。其优点是便于分离及纯化。同时对各晶型的获得及晶型间的相互转化进行了研究，并以Ｘ－射线粉末衍射及ＦＴ－ＩＲ进行了表征，并记录了不同晶型的酞菁氧钛在室温硫化硅橡胶中的吸收光谱。
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| 关 键 词： | 酞菁氧钛，合成，晶型，有机光导材料 |
| 收稿时间： | 1992-12-30 |
An Improved Method for Oxotitanium Phthalocyanine Preparation |
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| Wang Zhuting,Lu Kaijuan,Wang Xiaojun and Bai Fenglian.An Improved Method for Oxotitanium Phthalocyanine Preparation[J].Chinese Journal of Applied Chemistry,1994,11(1):72-75. |
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| Authors: | Wang Zhuting Lu Kaijuan Wang Xiaojun and Bai Fenglian |
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| Abstract: | Oxotitanium phthalocyanine was synthesized from phthalonitrile and titanium te-trachloride in bicyclohexyl.It is much more convenient to separate and purify the productsby using bicyclohexyl as a solvent. Five polymorphs were obtained and characterized by X-ray powder diffractometry and FTIR spectroscopy. The absorption spectra of the poly-morphs in silicone rubbers were recorded. |
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| Keywords: | oxotitanium phthalocyanine synthesis crystal form organic photoconductor |
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