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2,4-二氯苯酚气相色谱的内标法测定
引用本文:刘斌,王京平,刘明亮,朱海明. 2,4-二氯苯酚气相色谱的内标法测定[J]. 光谱实验室, 2004, 21(3): 576-578
作者姓名:刘斌  王京平  刘明亮  朱海明
作者单位:盐城市环境监测中心站,江苏省,盐城市区文港北路;盐城师范学院化学系,江苏省,盐城市,224002
摘    要:邻苯二甲酸二甲酯作为内标物 ,乙酸酐作为衍生剂 ,气相色谱分离和测定 2 ,4 -二氯苯酚 ,检出限为 0 .2 mg/ L,相对标准偏差为 2 .97% ,结果令人满意。

关 键 词:气相色谱法  2  4-二氯苯酚  柱前衍生化  内标法
文章编号:1004-8138(2004)03-0576-03
修稿时间:2003-09-22

Determination of 2,4-Dichlophenol with Internal Standard Method by Gas Chromatography
LIU Bin WANG Jing-Ping a LIU Ming-Liang a ZHU Hai-Ming a. Determination of 2,4-Dichlophenol with Internal Standard Method by Gas Chromatography[J]. Chinese Journal of Spectroscopy Laboratory, 2004, 21(3): 576-578
Authors:LIU Bin WANG Jing-Ping a LIU Ming-Liang a ZHU Hai-Ming a
Abstract:Using acetic anhydride as derivative and o-dimethyl phthalate as internal standard compound, 2,4- dichlophenol was separated and determined by gas chromatography.The detection limit and the relative standard deviation are 0.2mg/L and 2.97%,respectively,and the results are satisfactory.
Keywords:Gas Chromatography  2  4-Dichlophenol  Derivative on Injection Before  Internal Standard Method.
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