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巯基棉分离富集、石英缝管FAAS法测定河水中痕量铋
引用本文:陈文君,乙小娟.巯基棉分离富集、石英缝管FAAS法测定河水中痕量铋[J].化学分析计量,2001,10(6):17-18.
作者姓名:陈文君  乙小娟
作者单位:张家港出入境检验检疫局,215633
摘    要:研究了巯基棉分离富集、单缝石英管FAAS法测定铋的最佳条件。以盐酸作介质,巯基棉富集铋的最佳吸附酸度为0.1-0.2mol/L(盐酸),定量洗脱酸度为2mol/L(盐酸)。该法用于测定水中痕量的铋,回收率为96%-102%,相对标准偏差为4.8%。

关 键 词:巯基棉  单缝石英管  火焰原子吸收法    河水  测定  痕量分析
修稿时间:2001年7月30日

DETERMINATION OF THE TRACE BISMUTH IN THE RIVER WATER BY FAAS WITH SLOTTED QUARTZ TUBE AFTER SEPARATION AND ENRICHMENT WITH SULHYDRYL COTTON
Chen Wenjun,Yi Xiaojuan.DETERMINATION OF THE TRACE BISMUTH IN THE RIVER WATER BY FAAS WITH SLOTTED QUARTZ TUBE AFTER SEPARATION AND ENRICHMENT WITH SULHYDRYL COTTON[J].Chemical Analysis And Meterage,2001,10(6):17-18.
Authors:Chen Wenjun  Yi Xiaojuan
Institution:Zhangjiagang Entry - Exit Inspection and Quarantine Bureau 215633
Abstract:The optimum condition for determination of the trace bismuth in the river water by FAAS with slotted quartz tube after separation and enrichment with sulhydryl cotton is studied. The bismuth is enriched when the concentration of hydrochloric acid is from 0.1 - 0.2 mol/L and eluted quantitatively with 2 mol/L hydrochloric acid. This method is used to determine the trace bismuth in water with the recovery of bismuth being 96% - 102% ,and the relative standard deviation is 4.8% .
Keywords:sulhydryl cotton  slotted quartz tube  FAAS  bismuth
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