| 无催化剂条件下经微波辐射一步合成9-芳基-3,4,5,6,7,9-六氢-1H-氧杂蒽-1,8(2H)-二酮 |
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| 引用本文： | 华国平,李团结,朱松磊,章晓镜. 无催化剂条件下经微波辐射一步合成9-芳基-3,4,5,6,7,9-六氢-1H-氧杂蒽-1,8(2H)-二酮[J]. 有机化学, 2005, 25(6): 716-719 |
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| 作者姓名： | 华国平 李团结 朱松磊 章晓镜 |
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| 作者单位： | 1. 徐州职业技术学院,徐州,221008
2. 徐州师范大学化学系,江苏省药用植物生物技术重点实验室,徐州,221009 |
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| 基金项目： | 国家自然科学基金，江苏省重点实验室基金，江苏省重点实验室基金 |
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| 摘 要： | 微波辐射下以芳醛、1,3-环己二酮为原料在无催化剂条件下合成了一系列9-芳基-3,4,5,6,7,9-六氢-1H-氧杂蒽-1,8(2H)-二酮, 该反应时间短、产率高、后处理方便、环境友好.
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| 关 键 词： | 芳醛 1,3-环己二酮 微波辐射 氧杂蒽 |
| 收稿时间： | 2004-07-01 |
| 修稿时间： | 2004-07-01 |
One-pot Synthesis of 9-Aryl-3,4,5,6,7,9-hexahydro-1H-xanthene- 1,8(2H)-dione under Microwave Irradiation without Catalyst |
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| HUA,Guo-Ping,LI,Tuan-Jie,ZHU,Song-Lei,ZHANG,Xiao-Jing. One-pot Synthesis of 9-Aryl-3,4,5,6,7,9-hexahydro-1H-xanthene- 1,8(2H)-dione under Microwave Irradiation without Catalyst[J]. Chinese Journal of Organic Chemistry, 2005, 25(6): 716-719 |
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| Authors: | HUA Guo-Ping LI Tuan-Jie ZHU Song-Lei ZHANG Xiao-Jing |
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| Affiliation: | ( Xuzhou Institute of Architectural Technology Xuzhou 221008)( Department of Chemistry, Xuzhou Normal University, Key Laboratory of Biotechnology onMedical Plant of Ji-angsu Province, Xuzhou 221009) |
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| Abstract: | A series of 9-aryl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-diones were synthesized using aromatic aldehyde and 1,3-cyclohexadione as starting materials under microwave irradiation without cata- lyst. The reactions were easily worked up with short time, high yield and environmental friendliness. |
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| Keywords: | aromatic aldehyde 1 3-cyclohexadione microwave irradiation xanthene |
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