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二苯胺甲烷磺酸盐催化合成丙酸异戊酯
引用本文:刘春生,罗根祥.二苯胺甲烷磺酸盐催化合成丙酸异戊酯[J].合成化学,2004,12(5):514-516.
作者姓名:刘春生  罗根祥
作者单位:辽宁石油化工大学石油化工学院,辽宁,抚顺,113001;辽宁石油化工大学石油化工学院,辽宁,抚顺,113001
摘    要:以二苯胺甲烷磺酸盐为催化剂,合成了丙酸异戊酯,考察了反应时间、催化剂用量、醇酸摩尔比等因素对酯化率的影响。结果表明,在最佳条件下,酯化率可达97.7%。

关 键 词:丙酸异戊酯  二苯胺甲烷磺酸盐  酯化
文章编号:1005-1511(2004)05-0514-03
修稿时间:2003年7月9日

Synthesis of iso-Amyl Propionate Catalyzed by Diphenylammonium Methanesulfonate
LIU Chun-sheng,LUO Gen-xiang.Synthesis of iso-Amyl Propionate Catalyzed by Diphenylammonium Methanesulfonate[J].Chinese Journal of Synthetic Chemistry,2004,12(5):514-516.
Authors:LIU Chun-sheng  LUO Gen-xiang
Abstract:iso-Amyl propionate was synthesized by the esterification of propanoic acid with WT5BX]iso-amyl alcohol using diphenylammonium methanesulfonate as a catalyst. The effect of different factors, such as reaction time, the amount of catalyst and the ratio of iso-amyl alcohol to propanoic acid on the yield of iso-amyl propionate were carefully studied. The experiment results showed that the esterification rate was 97.7% under optimal reaction conditions.
Keywords:iso-amyl propionate  diphenylammonium methanesulfonate  esterification
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