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Applying the Taguchi Robust Design to Optimization of the Experimental Conditions for Synthesis of Lead Chromate Nanorods
Authors:Seied Mahdi Pourmortazavi  Mehdi Rahimi-Nasrabadi
Affiliation:1. Faculty of Material and Manufacturing Technologies, Malek Ashtar University of Technology , Tehran , Iran;2. Department of Chemistry , Islamic Azad University , Varamin Pishva Branch , Varamin , Iran
Abstract:
Orthogonal array design was employed as statistical method for controllable, simple, and fast synthesis of highly uniform PbCrO4 nanorods by precipitation method. Lead chromate nanorods were synthesized by addition of lead solution to chromate reagent. Effect of reaction conditions on the width of lead chromate rods were quantitavely evaluated by analysis of variance. Finally, optimum conditions for synthesis of lead chromate nanorods by this simple and fast method were proposed. The results of analysis of variance showed that 0.001 mol/L lead and chromate ion concentrations are optimum conditions for producing lead chromate nanorods with 87 ± 15 nm width.
Keywords:Lead chromate  mixing  nanostructure  precipitation  statistical optimization
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