| 硫杂吡啶番的合成和X射线结构分析 |
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| 引用本文： | 吴品昌,史锐,方德宇,张晓丽. 硫杂吡啶番的合成和X射线结构分析[J]. 光谱实验室, 2014, 0(6): 704-707 |
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| 作者姓名： | 吴品昌 史锐 方德宇 张晓丽 |
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| 作者单位： | 辽宁中医药大学信息工程学院,沈阳市祟山东路79号110847 |
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| 摘 要： | 采用与文献不同的方法,在同一反应中同时得到了2,11-二硫[3．3]（3,5）吡啶番、2,11,20-三硫[3．3．3]（3,5）吡啶番和2,11,20,29-四硫[3．3．3．3]（3,5）吡啶番,通过^1H NMR、MS以及X射线晶体结构分析确定了其结构;丰富了吡啶番类化合物和与其形成配位化合物的结构和物性上的知识,为这些新型化合物的进一步研究提供了新的理论依据。
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| 关 键 词： | 硫杂吡啶番 合成 结构研究 |
Synthesis and X-Ray Crystal Structure Analysis of Thiapyridinophane |
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| WU Pin-Chang,SHI Rui,FANG De-Yu,ZHANG Xiao-Li. Synthesis and X-Ray Crystal Structure Analysis of Thiapyridinophane[J]. Chinese Journal of Spectroscopy Laboratory, 2014, 0(6): 704-707 |
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| Authors: | WU Pin-Chang SHI Rui FANG De-Yu ZHANG Xiao-Li |
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| Affiliation: | ( Information Engineering College of Liaoning University of Traditional Chinese Medicine, Shenyang 110847,P.R.China ) |
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| Abstract: | In this paper, it synthesized 2,11-Dithia[3.3]（3,5）pyridinophane, 2,11,20-Trithia [3.3.3]（3,5） pyridinophane and 2,11,20,29-Tetrathia[3.3.3.3]（3,5）pyridinophane at the same time through another alternative figure which is different from document. It studied their structures through ^1H NMR, MS, and X-Ray crystal structure analysis In addition, these studies enriched the knowledge about structure and physical properties of pyridinophane compounds and their coordination compounds. |
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| Keywords: | Thiapyridinophane Synthesis Structure Research |
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