Synthesis and Crystal Structure of (E)-1-(2,3-Dihydroxybenzlidene)-4,4-Dimethythiosemicarbazide |
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Authors: | Ajay Pal Singh Pannu Maninder Singh Hundal |
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Institution: | (1) Department of Chemistry, Guru Nanak Dev University, Amritsar, 143005, India; |
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Abstract: | Abstract The Schiff base C10H13N3O2S is monoclinic, having unit cell parameters a = 9.788(1) ?, b = 9.615(1) ?, c = 12.605(1) ?, β = 108.41(1)° and V = 1125.56(2) ?3 and belongs to P21/n
space group. The molecule is almost planar. The two hydroxyl groups present on the phenyl ring are involved in intermolecular
H-bonding, which results in the stacking of molecules in the anti-parallel fashion leading an interesting network of channels.
Besides this C–H⋯π and π–π (edge to edge) interactions appear to provide stability to the crystal lattice. |
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Keywords: | |
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