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| 新型2-(2-羧基苯基)咪唑[4,5-f][1,10]邻菲咯啉的合成及其荧光性能 | |
| 引用本文： | 聂旭亮,吴东平,吴苏琴,涂勇刚,温世和,温辉梁. 新型2-(2-羧基苯基)咪唑[4,5-f][1,10]邻菲咯啉的合成及其荧光性能[J]. 合成化学, 2012, 20(2): 207-209,213 |
| 作者姓名： | 聂旭亮 吴东平 吴苏琴 涂勇刚 温世和 温辉梁 |
| 作者单位： | 1. 江西农业大学化学系,江西南昌,330045 2. 江西农业大学食品系,江西南昌,330045 3. 南昌大学化学系,江西南昌,330047 |
| 基金项目： | 江西省教育厅青年科学基金资助项目，江西农业大学自然科学研究基金资助项目 |
| 摘 要： | 以1,10-邻菲咯啉和邻羧基苯甲醛为原料,经氧化和缩合反应合成了一种新型的桥连配体——2-(2-羧基苯基)咪唑[4,S-f][1,10]邻菲咯啉(1),其结构经1H NMR,IR,MS和元素分析表征.用FL研究了1的荧光性能,结果表明,1具有较强的荧光,发光纯度较好. |
| 关 键 词： | 1,10-邻菲咯啉 咪唑 合成 荧光性能 |
Synthesis and Fluorescence Property of 2-(2-Carboxylphenyl)-1H-imidazo [4,5-f] [1,10] phenanthroline |
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| NIE Xu-liang , WU Dong-ping , WU Su-qin , TU Yong-gang , WEN Shi-he , WEN Hui-liang. Synthesis and Fluorescence Property of 2-(2-Carboxylphenyl)-1H-imidazo [4,5-f] [1,10] phenanthroline[J]. Chinese Journal of Synthetic Chemistry, 2012, 20(2): 207-209,213 | |
| Authors: | NIE Xu-liang WU Dong-ping WU Su-qin TU Yong-gang WEN Shi-he WEN Hui-liang |
| Affiliation: | 2(a.Department of Chemistry;b.Department of Food,1.Jiangxi Agricultural University,Nanchang 330045,China; 2.Department of Chemistry,Nanchang University,Nanchang 330047,China) |
| Abstract: | A new briging ligand,2-(2-carboxylphenyl)-1H-imidazo [4,5-f] [1,10] phenanthroline(1),was synthesised by oxidation and condensation from 1,10-phenanthtoline and o-carboxylaldehyde.The structure was characterized by 1 H NMR,IR,MS and elemental analysis.Fluorescence property of 1 was investigated by FL.The results showed that 1 exhibited strong fluorescence and the luminescence putry was better. |
| Keywords: | 1,10-phenanthtoline imidazole synthesis fluorescence property |
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