| Synthesis and Crystal Structure of 5-N-i-Propyl-2- （ 2＇ -nitrobenzenesulfonyl） -glutamine |
| |
| 基金项目： | Supported by the National Natural Science Foundation of China（ Nos. 20432010, 20602021 ）. |
| |
| 摘 要： |
|
| 关 键 词： | 合成 晶体结构 5-N-i-丙基-2-（2＇-硝基苯磺酰基）-谷氨酸盐 X-射线分析 |
| 文章编号： | 1005-9040（2006）-06-760-03 |
| 收稿时间： | 2005-10-26 |
Synthesis and Crystal Structure of 5-N-i-Propyl-2-(2′-nitrobenzenesulfonyl) -glutamine |
| |
| Authors: | Yong-jun XIAO Jian-guo WANG Bao-lei WANG Zheng-ming LI Hai-bin SONG |
| |
| Institution: | aElemento-Organic Chemistry Institute, State Key Laboratory of Elemento-Organic Chemistry, Nankai University, Tianjin 300071, P. R. China |
| |
| Abstract: | The title compound, 5-N-i-propyl-2-(2′-nitrobenzenesulfonyl)-glutamine, was synthesized and its structure was confirmed by IR, MS, 1H NMR, and elemental analysis. The single crystal structure of the title compound was determined by X-ray diffraction. The crystal belongs to Monoclinic, space group P2 (1), with a = 0.69281(11) nm, b = 0.76508(12), c = 1.5843(3) nm,  = 90°, β = 90.941(3)°, γ = 90°, V = 0.8397(2) nm3, Z = 2, Dc = 1.477 g/cm3, μ = 0.236 mm-1, F(000) = 392, R = 0.0297, and wR = 0.0664. |
| |
| Keywords: | 5-N-i-Propyl-2-(2′-nitrobenzenesulfonyl) -glutamine Synthesis Crystal structure |
| 本文献已被 ScienceDirect 等数据库收录！ |
|
