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New data on the thermal analysis of diphasic mullite gel
Authors:A K Chakravortty
Institution:(1) Central Glass & Ceramic Research Institute, 700 032 Calcutta, India
Abstract:A diphasic mullite gel has been synthesized by using Ludox and Al(NO3)3-9H2O in ammoniacal solution. Both DTA and DDTA studies have been performed with a sensitive differential thermal analyzer system. Besides usual exotherm due to mullite formation, a pronounced exotherm between 800–1300°C has been noted. Considering previous XRD data, it is explained as due to formation of Si-Al spinel phase, which is subsequently transformed exothermally at sim1320°C to mullite.
Keywords:diphasic mullite gel  Si-Al spinel  mullite
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