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Ni-ZrO2纳米复合电铸层的制备及纳米颗粒分布均匀性研究
引用本文:张文峰,朱荻.Ni-ZrO2纳米复合电铸层的制备及纳米颗粒分布均匀性研究[J].人工晶体学报,2006,35(4):889-892.
作者姓名:张文峰  朱荻
作者单位:1. 苏州职业大学机电系,苏州,215011;南京航空航天大学机电学院,南京,210016
2. 南京航空航天大学机电学院,南京,210016
基金项目:江苏省自然科学基金重点资助项目(BK2004005),国防基础研究基金资助项目(J1500E002)
摘    要:研究了在复合电铸过程中,当其它工艺参数一定时,复合电铸层的沉积速率及其厚度随时间的变化趋势,以及复合电铸层表面微观形貌随电沉积时间的变化趋势。测定了复合电铸层的组织成分,并就纳米颗粒在复合电铸层表面和横截面上分布的均匀性进行了评价。结果表明,复合电铸层表面平整,组织均匀致密,其组成主要是镍和所复合的纳米颗粒,纳米颗粒较为均匀地分散在复合电铸层中。

关 键 词:复合电铸  纳米颗粒  表面形貌  组织成分  分布均匀性
文章编号:1000-985X(2006)04-0889-04
收稿时间:09 7 2005 12:00AM
修稿时间:2005-09-07

Preparation of Ni-ZrO2 Nano-composite Electroforming Deposits and Research of Distribution of Nanoparticles
ZHANG Wen-feng,ZHU Di.Preparation of Ni-ZrO2 Nano-composite Electroforming Deposits and Research of Distribution of Nanoparticles[J].Journal of Synthetic Crystals,2006,35(4):889-892.
Authors:ZHANG Wen-feng  ZHU Di
Institution:1. Department of Mechanical and Electrical Engineering, Suzhou Vocational College, Suzhou 215011, China; 2. College of Mechanical and Electrical Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
Abstract:In the composite electroforming,when other process parameters were remained stationary,the variable tendency of codeposition rate and thickness of nano-composite electroforming deposits were investigated.SEM and EDS were used for the examination of surface morphology and the component of nano-composite electroforming deposits.Distribution of nanoparticles in surface and cross-section of nano-composite electroforming deposits was surveyed.Results indicate that the nano-composite electroforms composed by matrix metal Ni and ZrO_2 nanoparticles exhibit a smooth surface and compact microstructure,the nanoparticles are dispersed inside the metallic matrix.
Keywords:composite-electroforming  nanoparticle  surface morphology  structure content  uniformity
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