| EXPERIMENT TECHNIQUE RESEARCH OF SINGLE CRYSTAL X-RAY DIFFRACTION UNDER HIGH PRESSURE |
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| 引用本文： | 樊玉国,于景生,孟悦,徐义秋,邹广田. EXPERIMENT TECHNIQUE RESEARCH OF SINGLE CRYSTAL X-RAY DIFFRACTION UNDER HIGH PRESSURE[J]. 中国科学B辑(英文版), 1990, 0(8) |
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| 作者姓名： | 樊玉国 于景生 孟悦 徐义秋 邹广田 |
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| 作者单位： | Institute of Theoretical Chemistry，Jilin University，Jilin 130023，PRC，Institute of Theoretical Chemistry，Jilin University，Jilin 130023，PRC，Institute of Atomic and Molecular Physics，Jilin University，Jilin 130023，PRC，Institute of Atomic and Molecular Physics，Jilin University，Jilin 130023，PRC，Institute of Atomic and Molecular Physics，Jilin University，Jilin 130023，PRC |
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| 基金项目： | Project supported by the National Natural Science Foundation of China. |
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| 摘 要： | ![]()
We have set up the high pressure device used for single crystal X-ray diffraction, determined the X-ray absorption curve of the device on Nicolet four-circle diffractometer, established the data collection programme of a fixed φ scheme, and corrected the offsets of the optical centering of the crystal by using a reflection which is measured in eight different orientations. The mixture ratio of methanol: ethanol: water 16: 3: 1 was used as a pressure medium, high pressure calibration was based on the wavelength shift of the R_1 fluorescence line of ruby, and the pressure of 100 kbar was obtained.
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EXPERIMENT TECHNIQUE RESEARCH OF SINGLE CRYSTAL X-RAY DIFFRACTION UNDER HIGH PRESSURE |
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| FAN YU-GUO YU JING-SHENG. EXPERIMENT TECHNIQUE RESEARCH OF SINGLE CRYSTAL X-RAY DIFFRACTION UNDER HIGH PRESSURE[J]. Science in China(Chemistry), 1990, 0(8) |
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| Authors: | FAN YU-GUO YU JING-SHENG |
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| Abstract: | ![]()
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| Keywords: | high pressure diffraction different orientations reciprocal space |
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