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Analysis of nickel-niobium alloys by inductively coupled plasma optical emission spectrometry
Authors:de Lima Belmira B  Conte Rosa A  Nunes Carlos A
Affiliation:Faculdade de Engenharia Quimica de Lorena, Departamento de Engenharia de Materiais, Polo Urbo-Industrial, CP 116, CEP 12600-000, Lorena, S?o Paulo, Brazil.
Abstract:Inductively coupled plasma optical emission spectrometry (ICP-OES) was applied to the analysis of major and minor elements of Ni-Nb alloys obtained by aluminothermic reduction process. Digestion of samples was made using a mixture of HF+HNO3. Minor and trace elements were determined without matrix separation. The precision for all constituents was <3%. Recoveries for the analyte-spiked samples were 95%.
Keywords:Nickel-niobium alloys   Inductively coupled plasma optical emission spectrometry   Major elements   Minor elements
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