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Sulfamic acid immobilized on amino‐functionalized magnetic nanoparticles: A new and active magnetically recoverable catalyst for the synthesis of N‐heterocyclic compounds
Authors:Lotfi Shiri  Hojatollah Narimani  Mosstafa Kazemi
Affiliation:Department of Chemistry, Faculty of Basic Sciences, Ilam University, Ilam, Iran
Abstract:Sulfamic acid immobilized on amino‐functionalized magnetic nanoparticles (MNPs/DETA‐SA) was successfully fabricated and characterized using various techniques. Diameters of approximately 15 nm for the MNPs/DETA‐SA were observed from scanning electron microscopy images. The as‐fabricated nanocomposite was applied as an efficient and magnetically reusable catalyst for the synthesis of 2,3‐dihydroquinazoline‐4(1H)‐one and polyhydroquinoline derivatives. All products were obtained in good to excellent yields. Recovery tests confirm that the catalyst can be readily recovered using an external magnet and reused many times without significant loss of its catalytic activity.
Keywords:2,3‐dihydroquinazoline‐4(1H)‐one  magnetically reusable catalyst  MNPs/DETA‐SA  polyhydroquinolines
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