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| 流动注射化学发光法测定安痛定注射液中的氨基比林 | |
| 引用本文： | 何云华,聂峰,吕九如.流动注射化学发光法测定安痛定注射液中的氨基比林[J].分析化学,2001,29(3):296-298. |
| 作者姓名： | 何云华 聂峰 吕九如 |
| 作者单位： | 1. 汉中师范学院化学系, 2. 聊城师范学院化学系, 3. 陕西师范大学化学系, |
| 摘 要： | 在甲醛存在下 ,高锰酸钾与氨基比林能够发生化学发光反应 ,产生很强的化学发光 ,据此采用流动注射技术建立了一种测定氨基比林的化学发光分析法。方法的检出限为 3 .0× 10 -8g/mL ,相对标准偏差为 1.3 % (4 .0× 10 -6g/mL氨基比林 ,n =11) ,线性范围为 1.0× 10 -7～ 8.0× 10 -5g/mL氨基比林。该法已用于安痛定注射液中氨基比林含量的测定。 |
| 关 键 词： | 化学发光分析 高猛酸钾 氨基比林 流动注射 解热镇痛药 安痛定注射液 含量测定 |
Flow Injection-Chemiluminescence Determination ofAmidopyrine in the Antondin Injection |
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| HE Yunhua,Nie Feng,Lü Jiuru.Flow Injection-Chemiluminescence Determination ofAmidopyrine in the Antondin Injection[J].Chinese Journal of Analytical Chemistry,2001,29(3):296-298. | |
| Authors: | HE Yunhua Nie Feng Lü Jiuru |
| Abstract: | The chemiluminescence reaction of amidopyrine-potassium permanganate with formaldehyde as an enhancer was investigated by flow injection system. A method for the determination of amidopyrine on the basis of this technique was proposed. The detection limit is 3.0×10－8 g/mL, the relative standard deviation is 1.3% (4.0×10－6 g/mL amidopyrine,n=11).The linear range is 1.0×10－7～8.0×10－5g/mL amidopyrine. The method has been applied to the determination of amidopyrine in the antondin injection. |
| Keywords: | Chemiluminescence analysis potassium permanganate amidopyrine flow injection |
| 本文献已被 CNKI 万方数据 等数据库收录！ | |