| Using the Chiral Organophosphorus Derivatizing Agents for Determination of the Enantiomeric Composition of Chiral Carboxylic Acids by ^31PNMR Spectroscopy |
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| 引用本文： | ChaoCHE ZhongNingZHANG GuiLanHUANG XinXingWANG ZhaoHaiQIN. Using the Chiral Organophosphorus Derivatizing Agents for Determination of the Enantiomeric Composition of Chiral Carboxylic Acids by ^31PNMR Spectroscopy[J]. 中国化学快报, 2004, 15(6): 675-678 |
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| 作者姓名： | ChaoCHE ZhongNingZHANG GuiLanHUANG XinXingWANG ZhaoHaiQIN |
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| 作者单位： | [1]StateKeyLaboratoryofIntegtatedManagementofInsectsandRodents,Instituteofzoology,ChineseAcadamyofSciences,Beijing100080 [2]TheSixthResearchCenter,InstituteofChemicalDefenee,Beijing102205 [3]DepartmentofAppliedChemistry,ChinaAgriculturalUniversity,Beijing100094 |
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| 摘 要： | The use of chiral organophosphorus derivatizing agents prepared in situ from chiral tartrate or chiral diamine for the ^31PNMR determination of the enantiomeric composition of chiral carboxylic acids is described. The method is accurate, reliable and convenient.
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| 关 键 词： | 手性羧酸 核磁共振磷谱 手性酒石酸盐 手性二胺 光学异构体 |
Using the Chiral Organophosphorus Derivatizing Agents for Determination of the Enantiomeric Composition of Chiral Carboxylic Acids by 31PNMR Spectroscopy |
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| Chao CHE,Zhong Ning ZHANG,Gui Lan HUANG,Xin Xing WANG,Zhao Hai QINState Key Laboratory of Integrated Management of Insects and Rodents. Using the Chiral Organophosphorus Derivatizing Agents for Determination of the Enantiomeric Composition of Chiral Carboxylic Acids by 31PNMR Spectroscopy[J]. Chinese Chemical Letters, 2004, 15(6): 675-678 |
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| Authors: | Chao CHE Zhong Ning ZHANG Gui Lan HUANG Xin Xing WANG Zhao Hai QINState Key Laboratory of Integrated Management of Insects Rodents |
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| Affiliation: | Chao CHE,Zhong Ning ZHANG,Gui Lan HUANG,Xin Xing WANG,Zhao Hai QINState Key Laboratory of Integrated Management of Insects and Rodents,Institute of zoology,ChineseAcadamy of Sciences,Beijing 100080Graduate School of the Chinese Academy of Sciences,Beijing 100039The Sixth Research Center,Institute of Chemical Defence,Beijing 102205Department of Applied Chemistry,China Agricultural University,Beijing 100094 |
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| Abstract: | The use of chiral organophosphoras derivatizing agents prepared in situ from chiral tartrate or chiral diamine for the 31PNMR determination of the enantiomeric composition of chiral carboxylic acids is described. The method is accurate, reliable and convenient. |
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| Keywords: | Chiral tartrate chiral diamine enantiomeric composition determination 31PNMR carboxylic acids. |
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