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一种新型的空心镍纳米球的合成
引用本文:胡永红,容建华,刘应亮.一种新型的空心镍纳米球的合成[J].无机化学学报,2006,22(2):293-297.
作者姓名:胡永红  容建华  刘应亮
作者单位:暨南大学化学系,广州,510632
基金项目:广东省教育厅"人才引进工程"基金;广东省科技计划;广东省博士启动基金
摘    要:通过以二氧化硅粒子作为模板和金纳米粒子为表面晶种的方法制备了壳厚度可控的镍空心球。采用TEM﹑XRD对二氧化硅/镍复合球和镍空心球进行了表征和研究。结果表明镍纳米壳是由似针状的面心立方的镍纳米粒子构成的,碱溶液处理过程不影响镍纳米壳的形貌。高温处理显示镍空心球具有良好的热稳定性。

关 键 词:二氧化硅    金纳米粒子    镍纳米粒子    空心球
文章编号:1001-4861(2006)02-0293-05
收稿时间:2005-09-19
修稿时间:2005-11-21

Synthesis of Novel Nickel Hollow Nanospheres
HU Yong-Hong,RONG Jian-Hua and LIU Ying-Liang.Synthesis of Novel Nickel Hollow Nanospheres[J].Chinese Journal of Inorganic Chemistry,2006,22(2):293-297.
Authors:HU Yong-Hong  RONG Jian-Hua and LIU Ying-Liang
Institution:Department of Chemistry, Jinan University, Guangzhou 510632,Department of Chemistry, Jinan University, Guangzhou 510632 and Department of Chemistry, Jinan University, Guangzhou 510632
Abstract:he hollow nickel spheres with controllable shell thickness were prepared by using silica particles as templates and Au-surface seeding method. The nickel-coated silica spheres and the hollow nickel spheres were characterized by transmission electron microscopy (TEM), X-ray diffraction (XRD). The results showed that the nickel shells were consisted of face-centered cubic needlelike nickel particles, and the morphology of the nickel shells was not changed after treatment in alkaline solution. The hollow nickel spheres exhibits good heat stability.
Keywords:silica  Au nanoparticles  nickel nanoparticles  hollow spheres
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