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Rapid Synthesis of Lead Oxide Nanorods by One-step Solid-state Chemical Reaction at Room Temperature
作者姓名:曹亚丽  贾殿赠  刘浪  骆建敏
作者单位:[1]InstituteofAppliedChemistry,XinjiangUniversity,Urumqi,Xinjiang830046,China [2]PhysicsandChemistryDetectingCenterofXinjiangUniversity,Urumqi,Xinjiang830046,China
基金项目:Project supported by the National Natural Science Foundation of China (Nos. 20161003,20262005).
摘    要:A simple and facile method was reported to synthesize lead oxide nanorods. Nanorods of lead oxide were obtained directly from grinding solid metal salt and sodium hydroxide in agate mortar with the assistance of a suitable nonionic surfactant in only one step, which is different from the result of hydroxide in solution. The product has been characterized by XRD, TEM and SEM. The formation mechanism of rod-like morphology is discussed and the surfactant plays an important soft-template role in modifying the interface of solid-state reaction and according process of rod-formation.

关 键 词:合成  纳米材料  铅氧化物  固态化学反应  室温

Rapid Synthesis of Lead Oxide Nanorods by One-step Solid-state Chemical Reaction at Room Temperature
CAO,Ya-Lia JIA,Dian-Zeng,aLIU,Langa LUO,Jian-Minb a Institute of Applied Chemistry,Xinjiang University,Urumqi,Xinjiang ,China b Physics and Chemistry Detecting Center of Xinjiang University,Urumqi,Xinjiang ,China.Rapid Synthesis of Lead Oxide Nanorods by One-step Solid-state Chemical Reaction at Room Temperature[J].Chinese Journal of Chemistry,2004,22(11):1288-1290.
Authors:CAO  Ya-Lia JIA  Dian-Zeng  aLIU  Langa LUO  Jian-Minb a Institute of Applied Chemistry  Xinjiang University  Urumqi  Xinjiang  China b Physics and Chemistry Detecting Center of Xinjiang University  Urumqi  Xinjiang  China
Institution:CAO,Ya-Lia JIA,Dian-Zeng*,aLIU,Langa LUO,Jian-Minb a Institute of Applied Chemistry,Xinjiang University,Urumqi,Xinjiang 830046,China b Physics and Chemistry Detecting Center of Xinjiang University,Urumqi,Xinjiang 830046,China
Abstract:A simple and facile method was reported to synthesize lead oxide nanorods. Nanorods of lead oxide were obtained directly from grinding solid metal salt and sodium hydroxide in agate mortar with the assistance of a suitable nonionic surfactant in only one step, which is different from the result of hydroxide in solution. The product has been characterized by XRD, TEM and SEM. The formation mechanism of rod-like morphology is discussed and the surfactant plays an important soft-template role in modifying the interface of solid-state reaction and according process of rod-formation.
Keywords:nanomaterial  nanorod  lead oxide  solid-state reaction  
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