| Synthesis and Crystal Structure of 1-Phenyl-3-methyl-4-（4-bromophenyl）-6-（2-chlorophenyl）-pyrazolo[3,4-b] Pyridine under Microwave Irradiation |
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| 引用本文： | 邹翔,屠树江,朱松磊,纪顺俊,张勇.Synthesis and Crystal Structure of 1-Phenyl-3-methyl-4-（4-bromophenyl）-6-（2-chlorophenyl）-pyrazolo[3,4-b] Pyridine under Microwave Irradiation[J].结构化学,2005,24(1):109-113. |
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| 作者姓名： | 邹翔 屠树江 朱松磊 纪顺俊 张勇 |
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| 作者单位： | ZOU Xianga，c ZHU Song-Leia (Department of Chemistry，Xuzhou Normal University，Xuzhou，Jiangsu 221009，China) (Lianyungang Teacher's College，Lianyungang，Jiangsu 222000，China) JI Shun-Jun ZHANG Yong (College of Chemistry and Chemical Engineering，Key Lab. of Org. Synth. of Jiangsu Province，Suzhou University，Jiangsu 215006，China) |
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| 基金项目： | The project was supported by the National Natural Science Foundation of China (No. 20372057)，Natural Science Foundation of Jiangsu Province (No. BK.2001142)，the Open-end Fund of the Key Experiments of Organic Synthesis，Jiangsu Province (S8109111) and the Fund of Jiangsu Provincial Key Lab of Biotechnology for Medicinal Plants (01AXL 14) |
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| 摘 要： | 1INTRODUCTIONThepyrazolo3,4-b]pyridineclassofcompoundspossessmanybiologicalandpharmacologicalactivi-ties1],suchasactiveanti-concretionmedicaments2]aswellasactiveanti-gramnegativeandpositivebacteriaagents3].Thereforethesynthesesofsuchcompoundshavearousedgreatattentionofalargenumberofchemists.Themostimportantsyntheticrouteisthecondensationreaction4～11]ofamino-pyrazoleandα,β-unsaturatedcompounds.Theorganicreactionundermicrowaveirradia-tionhastheadvantagesoffastreactionspeed,shorttime…
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| 关 键 词： | 合成 晶体结构 1-苯基-3-甲基-4-（4-溴苯基）-6-（2-氯苯基）-吡唑[3 4-b]嘧啶 微波照射 |
Synthesis and Crystal Structure of 1-Phenyl-3-methyl-4-(4-bromophenyl)-6-(2-chlorophenyl)-pyrazolo[3,4-b] Pyridine under Microwave Irradiation |
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| ZOU Xiang,TU Shu-Jiang,ZHU Song-Lei,JI Shun-jun,ZHANG Yong.Synthesis and Crystal Structure of 1-Phenyl-3-methyl-4-(4-bromophenyl)-6-(2-chlorophenyl)-pyrazolo[3,4-b] Pyridine under Microwave Irradiation[J].Chinese Journal of Structural Chemistry,2005,24(1):109-113. |
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| Authors: | ZOU Xiang TU Shu-Jiang ZHU Song-Lei JI Shun-jun ZHANG Yong |
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| Institution: | Department of Chemistry, Xuzhou Normal University, Xuzhou, Jiangsu 221009, China;Lianyungang Teacher's College, Lianyungang, Jiangsu 222000, China;Department of Chemistry, Xuzhou Normal University, Xuzhou, Jiangsu 221009, China;College of Chemistry and Chemical Engineering, Key Lab.of Org.Synth.of Jiangsu Province, Suzhou University, Jiangsu 215006, China |
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| Abstract: | The title compound (C25H17BrC1N3) has been synthesized by the reaction of 1-(2-chlorophenyl)-3-(4-bromophenyl)-2-propylene-1-one with 5-amino-3-methyl-1-phenyl-5-pyrazole under microwave irradiation and its structure was determined by single-crystal X-ray diffraction. |
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| Keywords: | aminopyrazole pyrazolopyridine crystal structure microwave irradiation |
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