| Fe2(MoO4)3超细微粒催化剂的制备 |
| |
| 引用本文： | 匡文兴,范以宁,陈开东,王净雷,陈懿.Fe2(MoO4)3超细微粒催化剂的制备[J].物理化学学报,1997,13(1):86-88. |
| |
| 作者姓名： | 匡文兴 范以宁 陈开东 王净雷 陈懿 |
| |
| 作者单位： | Department of Chemistry,Nanjing University,Nanjing 210093 |
| |
| 基金项目： | 国家自然科学基金，85－06NMS资助 |
| |
| 摘 要： | 近年来，超细微粒因其具有明显的体积效应和表面效应已被广泛应用于陶瓷、光学、电磁、生物、染料、医药、农业等领域［‘，‘l其中复合氧化物超细微粒是近年来国内外正致力开发的一种新型催化材料，有关这类材料的制备、表征和催化性能的研究有重要的理论和实际意义．文献报导
|
| 关 键 词： | Fe2(MoO4)3 超细微粒 溶胶-凝胶法 |
| 收稿时间： | 1996-06-28 |
| 修稿时间： | 1996-10-11 |
Preparation of Fe_2(MoO_4)_3 Ultrafine Particle Catalyst |
| |
| Kuang Wenxing, Fan Yining,Chen Kaidong,Wang Jinglei,Chen Yi.Preparation of Fe_2(MoO_4)_3 Ultrafine Particle Catalyst[J].Acta Physico-Chimica Sinica,1997,13(1):86-88. |
| |
| Authors: | Kuang Wenxing Fan Yining Chen Kaidong Wang Jinglei Chen Yi |
| |
| Institution: | Department of Chemistry,Nanjing University,Nanjing 210093 |
| |
| Abstract: | Fe2(MoO4)3 ultrafine particle catalyst has been prepared successfully by the sol-gel process at lower temperature. The influences of preparation conditions and thermal treatment conditions on the morphology and structure of the ultrafine particle catalyst has been studied by using TEM, DTA-TG, FT-IR, XRD and BET surface area measurement methods. It is shown that the BET surface area of Fe2(MoO4)3 ultrafine particle prepared by sol-gel method is much larger than that of Fe2(MoO4)3 prepared by coprecipitation method. For the preparation of the welldistribuated Fe2(MoO4)3 ultrafine particles with the size in the range of 40-80nm, the optimumconditions are : treatment temperature <673K, L/M (Citric acid/Metallic ions)=0.3 and pH<1 .0. |
| |
| Keywords: | Fe_2(MoO_4 )_3 Ultrafine particle Sol-gel method |
| 本文献已被 CNKI 维普 等数据库收录！ |
| 点击此处可从《物理化学学报》浏览原始摘要信息 |
| 点击此处可从《物理化学学报》下载免费的PDF全文 |
|
