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硫酸镍中Ca,Mg,Cu,Fe,Pb,Zn的光谱测定
引用本文:王民贤.硫酸镍中Ca,Mg,Cu,Fe,Pb,Zn的光谱测定[J].化学分析计量,2000,9(1):18-19.
作者姓名:王民贤
作者单位:国营755厂 新乡
摘    要:用发射光谱法测定结晶硫酸镍中Ca,Mg,Cu,Fe,Pb,Zn等杂质元素,加入NaCl为缓冲剂改善杂质元素的激发行为,以提高分析的灵敏度。用交流电弧激发,以镍为内标,一次摄谱,可同时测定上述六种元素。此法快速、准确,满足实际需要。

关 键 词:发射光谱法  硫酸镍  缓冲剂  交流电弧  杂质元素

DETERMINATION OF Ca,Mg,Cu,Fe,Pb AND Zn IN NICKEL SULFATE BY AES
Wang Minxian.DETERMINATION OF Ca,Mg,Cu,Fe,Pb AND Zn IN NICKEL SULFATE BY AES[J].Chemical Analysis And Meterage,2000,9(1):18-19.
Authors:Wang Minxian
Abstract:The impurities of Ca,Mg,Cu,Fe,Pb and Zn in Nickel sulfate are determined by using emission spectrum under 5.5-6 A of current and 5 s of exposure time.Nickel is used as internal standard element and NaCl serves as spectral buffer.This method is proved as accurate,easy and quick.
Keywords:emission spectrum  nickel sulfate  buffer  alternating current arc  
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