| 含甲氧基二氮杂萘酮结构类双酚单体的波谱表征 |
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| 引用本文： | 靳焜,王沛,彭勤纪,蹇锡高. 含甲氧基二氮杂萘酮结构类双酚单体的波谱表征[J]. 波谱学杂志, 2006, 23(2): 193-198 |
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| 作者姓名： | 靳焜 王沛 彭勤纪 蹇锡高 |
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| 作者单位： | 大连理工大学,精细化工国家重点实验室;大连理工大学,高分子材料系,辽宁,大连,116012 |
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| 基金项目： | 国家自然科学基金资助项目(50143013) |
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| 摘 要： | 用核磁共振谱和质谱表征了4-（3-甲氧基-4-羟基苯基）-2,3-二氮杂萘-1-酮 (OO-DHPZ) ，对其结构的1H和13Ｃ NMR谱的化学位移作了全归属.
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| 关 键 词： | 核磁共振谱 甲氧基二氮杂萘酮 归属 质谱 |
| 文章编号： | 1000-4556（2006）02-0193-06 |
| 收稿时间： | 2005-09-08 |
| 修稿时间： | 2005-11-16 |
Characterization of Phthalazinone Moiety Containing Methoxyl Side Group by NMR Spectroscopy |
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| JIN Kun,WANG Pei,PENG Qin-ji,JIAN Xi-gao. Characterization of Phthalazinone Moiety Containing Methoxyl Side Group by NMR Spectroscopy[J]. Chinese Journal of Magnetic Resonance, 2006, 23(2): 193-198 |
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| Authors: | JIN Kun WANG Pei PENG Qin-ji JIAN Xi-gao |
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| Affiliation: | State Key Laboratory of Fine Chemicals; 2.Department of Polymer Science & Materials, Dalian, 116012 |
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| Abstract: | The structure of 4-(3-methoxyl-4-hydroxyphenyl)-phthalazin-1-one(OO-DPHZ) was determined by NMR spectroscopy and MS spectrometry.The ~1H and ~(13)C chemical shifts of the compound were assigned using two dimensional NMR spectroscopy,including gCOSY,gHSQC and gHMBC. |
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| Keywords: | NMR spectroscopy phthalazinone methoxyl group assignment MS spectrometry |
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