| 氧氟沙星在胶束体系中的荧光特性及应用 |
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| 引用本文： | 杜黎明,王静萍,范哲锋,叶玉香.氧氟沙星在胶束体系中的荧光特性及应用[J].分析化学,2002,30(1):59-61. |
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| 作者姓名： | 杜黎明 王静萍 范哲锋 叶玉香 |
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| 作者单位： | 山西师范大学分析测试中心,临汾,041004 |
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| 基金项目： | 山西省自然科学基金资助课题（No．2001 1016） |
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| 摘 要： | 研究发现十二烷基硫酸钠胶束对氧氟沙星荧光有明显的增敏作用，据此建立了直接测定人体尿液中氧氟沙星的等波长差同步荧光光谱法（△λ=90nm）。经样品测定，其线性范围为0．12－3．6mg/L，检出限为0．12mg/L，回收率为92．2％－97．8％，相对标准偏差为1．2％－2．7％。
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| 关 键 词： | 氧氟沙星 十二烷基硫酸钠 同步荧光光度法 抗菌药物 尿液 测定 增敏作用 分析 |
The Fluorescence Characteristics of Ofloxa cin in Micellar System and Its Application |
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| Du Liming,Wang Jingping,Fan Zhefeng,Ye Yuxiang.The Fluorescence Characteristics of Ofloxa cin in Micellar System and Its Application[J].Chinese Journal of Analytical Chemistry,2002,30(1):59-61. |
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| Authors: | Du Liming Wang Jingping Fan Zhefeng Ye Yuxiang |
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| Abstract: | The fluorescence characteristics of complexes of ofloxacin in micellar systems have been studied in details. The experiments indicate that sodium dodecyl sulfate micellar systems can enhance greatly the fluorescence signal. The pH value has an obvious effect and the maximum fluorescence signal can be obtained at pH 5.0. A new method using the synchronous fluorimetry has been developed for the detemiination of ofloxacin in human urine. The linear range was 0.12-3.6 mg/Land the detection limit was 0.12 mg/L, the RSD was 1.2% -2.7% and the recovery was within the range of 92.2% -97.8%. |
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| Keywords: | Ofloxacin sodium dodecyl sulfate synchrnnous fluorimetry |
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