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具有可见光催化活性的Ag_3PO_4/NaNbO_3复合材料的合成与表征
引用本文:常海波,杨磊飞,耿世杰,刘俊渤,唐姗姗,李婉莹.具有可见光催化活性的Ag_3PO_4/NaNbO_3复合材料的合成与表征[J].分子科学学报,2017,33(3).
作者姓名:常海波  杨磊飞  耿世杰  刘俊渤  唐姗姗  李婉莹
作者单位:吉林农业大学资源与环境学院,吉林长春,130118
基金项目:吉林大学无机合成与制备化学国家重点实验室开放课题,吉林农业大学博士启动基金
摘    要:采用共沉淀法制备了Ag_3PO_4/NaNbO_3复合半导体光催化剂,利用X-射线衍射、X射线光电子能谱、紫外漫反射和扫描电镜等方法对合成样品进行表征.测试了样品对亚甲基蓝溶液的光催化降解活性,复合材料的催化活性远高于单体的Ag_3PO_4和NaNbO_3.

关 键 词:NaNbO3  Ag3PO4  复合催化剂  可见光催化

Synthesis and characterization of Ag3PO4/NaNbO3 composite with enhance visible-light photocatalytic activity
CHANG Hai-bo,YANG Lei-fei,GENG Shi-jie,LIU Jun-bo,TANG Shan-shan,LI Wan-ying.Synthesis and characterization of Ag3PO4/NaNbO3 composite with enhance visible-light photocatalytic activity[J].Journal of Molecular Science,2017,33(3).
Authors:CHANG Hai-bo  YANG Lei-fei  GENG Shi-jie  LIU Jun-bo  TANG Shan-shan  LI Wan-ying
Abstract:Ag3PO4/NaNbO3 composite photocatalytic material was prepared by simple coprecipitation method.X-ray diffraction (XRD),X-ray photoelectron spectroscope (XPS),Scan electron microscope (SEM) and UV-Vis diffusion reflectance spectra (DRS) were employed to characterize the composition.The photocatalytic activity of Ag3 PO4/NaNbO3 was investigated by simulation of methylene blue (MB) dye pollutants under the xenon lamp (220 V,350 W) conditions.The higher photocatalytic activity of Ag3 PO4/NaNbO3 was attributed to the synergistic effects of more visible light absorption and minimum electron hole recombination.The experimental results show that the composite of Ag3PO4/ NaNbO3 catalyst with molar ratio 4 ∶ 1 exhibited the highest degradation efficiency.The degradation rate of half an hour reached to 92.4%.
Keywords:NaNbO3  Ag3PO4  composite  visible light catalysis
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