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Controlled Synthesis and Electrochemical Behavior of Single-crystal MoO2 Nanowhiskers by a Facile Precursor-reduction Route
引用本文:Yu Mei KONG Jun PENG Feng Shan SHEN Bao Xia DONG Li Ll. Controlled Synthesis and Electrochemical Behavior of Single-crystal MoO2 Nanowhiskers by a Facile Precursor-reduction Route[J]. 中国化学快报, 2006, 17(6): 825-828
作者姓名:Yu Mei KONG Jun PENG Feng Shan SHEN Bao Xia DONG Li Ll
作者单位:Yu Mei KONG,Jun PENG,Feng Shan SHEN,Bao Xia DONG,Li LI Key Laboratory of Polyoxometalate Science of Ministry of Education,Faculty of Chemistry,Northeast Normal University,Changchun 130024
摘    要:Among the transition-metal oxides, molybdenum oxides are the focus of much attention owing to its numerous applications in catalysts, additives, sensors, photochromic and electrochromic materials1. Especially, the applications of MoO2 in optical propertie…

关 键 词:合成方法 表征 电气化学 MoO2 单晶结构 二氧化钼 纳米晶须
收稿时间:2003-12-13

Controlled Synthesis and Electrochemical Behavior of Single-crystal MoO2 Nanowhiskers by a Facile Precursor-reduction Route
Yu Mei KONG,Jun PENG,Feng Shan SHEN,Bao Xia DONG,Li LI. Controlled Synthesis and Electrochemical Behavior of Single-crystal MoO2 Nanowhiskers by a Facile Precursor-reduction Route[J]. Chinese Chemical Letters, 2006, 17(6): 825-828
Authors:Yu Mei KONG  Jun PENG  Feng Shan SHEN  Bao Xia DONG  Li LI
Abstract:A novel method for controlled synthesis of crystalline molybdenum dioxides nanowhiskers (whisker-MoO2) by using moderate reductive and precursor ion under hydrothermal conditions is reported. The result shows that the as-obtained samples have a monoclinic structure, and the whisker-MoO2 is composed of nanowires with diameters of ca. 20 nm. Formation of whisker-MoO2 was through a typical precursor-reduction process, in which cetyltrimethylammonium bromide (CTAB) served as a cationic surfactant and acetone as a reductant. The electrochemical behavior of whisker-MoO2 was studied.
Keywords:Synthetic methods   characterization   MoO2 nanowhiskers   electrochemical behavior.
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