A fast, simple calibration method for organic carbon isotope analysis using continuous-flow elemental analyzer interfaced with an isotope ratio mass spectrometer. |
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Authors: | Yeon-Sik Bong Kwang-Sik Lee |
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Affiliation: | Division of Isotope Geoscience, Korea Basic Science Institute, 52 Eoeun-dong, Yusung-gu, Daejeon 305-333, Korea. |
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Abstract: | Continuous flow analysis using an elemental analyzer interfaced with an isotope ratio mass spectrometer (EA-IRMS) is faster and requires much less material than conventional analytical methods. Although using an EA-IRMS is simple and fast, accurate calibration strongly depends on matching sample and reference peak heights by adjusting the sample weight. This paper describes a new modification for calibration using only the major ion beam intensity (nA) without weighing each sample or increasing the number of reference materials. |
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