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High oxygen vacancy tin oxide synthesized by combustion chemical vapor deposition (CCVD)
Authors:Qi‐Hui Wu  Jie Song  Jincai Li
Institution:1. Department of Physics, Xiamen University, Xiamen 361005, China;2. Department of Chemistry, Xiamen University, Xiamen 361005, China
Abstract:Tin oxide nanotentacles were synthesized by combustion chemical vapor deposition in air. Their surface composition and optical properties were then investigated using X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy. XPS core level spectra indicate that these nanotentacles are of high oxygen vacancy with chemical composition of about SnO1.6, which is also supported by the Sn Auger parameter. Besides SnO2, the optical properties of SnO were detected in Raman spectrum. Moreover, two new Raman peaks were found for the SnO2 phase because of the high oxygen vacancy concentration. Copyright © 2008 John Wiley & Sons, Ltd.
Keywords:tin oxides  nanotentacles  CCVD
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