Development of an automated in situ fracture stage for a ToF‐SIMS system |
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| Authors: | Arran R. Wood Nicolas Benedetto Nigel Hooker Edward Scullion Paul A. Smith John F. Watts |
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| Affiliation: | Surrey Materials Institute and Faculty of Engineering and Physical Sciences, University of Surrey, Guildford, Surrey, GU2 7XH, UK |
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| Abstract: | The design philosophy and implementation of an ultra high vacuum (UHV), PC controlled, automated in situ fracture stage for a surface analysis system is described. ToF‐SIMS spectra are shown to illustrate the improvement in spectral quality obtained from micro‐compact tension (CT) tests of polymer matrix fracture surfaces produced using the fracture stage in UHV compared to those obtained from a sample tested at air. This system is flexible in that by changing the capacity of the load cell it is possible to reduce or increase maximum loads as the specimen type and material demands. The stage has been designed with instrumental flexibility in mind, utilising commercial SEM‐stub type sample mounts, and can thus be used for AES/SAM and XPS investigations, as well as ToF‐SIMS analysis, in the authors' laboratory. Copyright © 2008 John Wiley & Sons, Ltd. |
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| Keywords: | ToF‐SIMS in situ fracture composite materials |
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