| 柴油中硫成分分析系列标准物质的研制 |
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| 引用本文： | 史乃捷,李云巧,侯云艳,卢晓华,刘孟刚,王东东,姬建民.柴油中硫成分分析系列标准物质的研制[J].化学分析计量,2003,12(4):1-3. |
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| 作者姓名： | 史乃捷 李云巧 侯云艳 卢晓华 刘孟刚 王东东 姬建民 |
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| 作者单位： | 国家标准物质研究中心,北京,100013 |
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| 摘 要： | 介绍柴油中硫成分分析系列标准物质的研制过程，选择低硫成分的直馏柴油作为基体材料制备柴油中硫成分分析系列标准物质，采用X射线能量色散荧光光谱法进行均匀性检验、氧弹燃烧-离子色谱法进行稳定性监测、5种不同原理的测量方法进行定值。给出了柴油中硫成分分析系列标准物质的标准值和扩展不确定度。
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| 关 键 词： | 柴油 硫 成分分析 标准物质 研制 X射线能量色散荧光光谱法 均匀性检验 |
| 修稿时间： | 2003年4月28日 |
DEVELOPMENT OF SERIES OF CERTIFIED REFERENCE MATERIALS OF SULFUR IN DIESEL OIL |
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| Shi Naijie,Li Yunqiao,Hou Yunyan,Lu Xiaohua,Liu Menggang,Wang Dongdong,Ji Jianmin.DEVELOPMENT OF SERIES OF CERTIFIED REFERENCE MATERIALS OF SULFUR IN DIESEL OIL[J].Chemical Analysis And Meterage,2003,12(4):1-3. |
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| Authors: | Shi Naijie Li Yunqiao Hou Yunyan Lu Xiaohua Liu Menggang Wang Dongdong Ji Jianmin |
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| Abstract: | The developing proccess of series of certified reference materials of sulfur in diesel oil was described. The series of certified reference materials of sulfur in diesel oil were prepared by using low sulfur straight-run diesel oil as matrix material, the homogeneities were tested by X ray energy dispersive fluorescence spectrometry, the stabilities were inspected by bomb-ion chromatography and the certifications were conducted by five kinds of difference principles methods of measurement. The certified values of sulfur and expand uncertainties of series of certified reference materials of sulfur in diesel oil were given. |
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| Keywords: | diesel sulfur certified reference material development |
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