Synthesis and structure of 2,2′-spirobi(1,3-benzodioxole) derivative prepared from 3,5-di(<Emphasis Type="Italic">tert</Emphasis>-butyl)-1,2-benzoquinone |
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| Authors: | V N Komissarov Yu A Sayapin V I Minkin V V Tkachev S M Aldoshin G V Shilov |
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| Institution: | (1) Institute of Physical and Organic Chemistry at Rostov State University, Rostov-on-Don, 344090, Russia;(2) Institute of Problems of Chemical Physics, Russian Academy of Sciences, Chernogolovka, Russia |
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| Abstract: | 3,5-Di(tert-butyl)-1,2-benzoquinone reacted with 1,2,3-trimethylbenzimidazolium iodide led to the formation of 2,2′-spirobi4,6-di(tert-butyl)-1,3-benzodioxole]. The reaction mechanism was suggested. The structure of 2,2′-spirobi4,6-di(tert-butyl)-1,3-benzodioxole] was established by means of X-ray diffraction analysis. |
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