| 1,2-二氢-4-(4-羟基苯基)(2H)二氮杂萘-1-酮的NMR研究 |
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| 引用本文： | 高红昌,方晓雯,张涛,程琳,袁汉珍,毛诗珍. 1,2-二氢-4-(4-羟基苯基)(2H)二氮杂萘-1-酮的NMR研究[J]. 波谱学杂志, 2001, 18(4): 343-349 |
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| 作者姓名： | 高红昌 方晓雯 张涛 程琳 袁汉珍 毛诗珍 |
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| 作者单位： | 中国科学院武汉物理与数学研究所,波谱与原子分子物理国家重点实验室,武汉,430071;武汉化工学院,武汉,430074 |
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| 基金项目： | 国家自然科学基金资助项目 (No .2 9874 0 38) |
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| 摘 要： | 应用多种二维核磁共振谱,即：2D同核化学位移全相关谱(TOCSY),2D NOESY谱,2D 异核多量子相关谱(HMQC)和2D异核13C-1H多键 相关谱(HMBC),对化合物1,2-二氢-4-(4-羟基苯基)(2H)二氮杂萘-1-酮的1H和13C NMR 谱线进行了完整归属,从而系统地分析和讨论了该化合物的结构特征.
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| 关 键 词： | NMR 二维核磁共振 二氮杂萘酮 归属 |
| 文章编号： | 1000-4556(2001)04-0343-7 |
| 收稿时间： | 2001-07-19 |
| 修稿时间： | 2001-07-19 |
NMR Studies for the 1,2-Dihydro-4-(4-Hydroxy-Phenyl)(2H)Phthalazine-1-One |
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| GAO Hong-chang ,FANG Xiao-wen ,ZHANG Tao ,CHENG Lin ,YUAN Han-zhen and MAO Shi-zhen. NMR Studies for the 1,2-Dihydro-4-(4-Hydroxy-Phenyl)(2H)Phthalazine-1-One[J]. Chinese Journal of Magnetic Resonance, 2001, 18(4): 343-349 |
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| Authors: | GAO Hong-chang FANG Xiao-wen ZHANG Tao CHENG Lin YUAN Han-zhen MAO Shi-zhen |
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| Affiliation: | 1.State Key Laboratory of Magnetic Resonance and Atomic and Molecular P hysics, Wuhan Institute of Physics and mathematics, The Chinese Academy of Sciences, Wuh an 430071; 2.Wuhan Institute of Chemical Technology, Laboratory of Advanced Aromatic Het erocyclic Materials, Wuhan 430074 |
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| Abstract: | By using two-dimensional NMR techniques, i.e. Total correlation spectroscopy (TOCSY), two-dimensional nuclear Overhauser enhancement (2D NOESY),two-dimensional heteronuclear multiple quantum coherence (HMQC) and two-dimensional heteronuclear multiple-bond correlation (HMBC), 1H and 13C NMR spectra of the compound 1,2-dihydro-4-(4-hydroxylphenyl)(2H) phthalazin- 1-one were completely assigned. The structural characteristics of the compound were analysed and discussed. |
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| Keywords: | NMR Two-dimensional NMR Phthalazinone Assignment |
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