Determination of strontium in human serum by inductively coupled plasma mass spectrometry and neutron activation analysis: A comparison |
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| Authors: | Vandecasteele C Vanhoe H Dams R Vanballenberghe L Wittoek A Versieck J |
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| Affiliation: | Laboratory for Analytical Chemistry, University of Ghent, Institute for Nuclear Sciences, Proeftuinstraat 86, B-9000 Ghent, Belgium. |
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| Abstract: | Strontium has been determined in a human serum reference material by ICP-MS and by NAA. By ICP-MS, results for (88)Sr and (86)Sr in both 10- and 5-fold diluted serum were in good agreement. For (88)Sr the precision was better than 3% and the detection limit was 0.05 mug/l. under the conditions used. The results were 25.5 mug/l. in the liquid serum or 0.281 mug/g in the lyophilized reference material. In the NAA the (87m)Sr produced was radiochemically separated by extraction with oxine in chloroform. The precision was about 10% and the detection limit 0.02-0.05 mug/g. |
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