An electrolytic device for preparation of hydrogen and oxygen from water for isotopic analysis |
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Authors: | Iqbal M S Rashid F Javed N A |
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Institution: | Nuclear Chemistry Division, Pakistan Institute of Nuclear Science and Technology, P.O. Nilore, Islamabad, Pakistan. |
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Abstract: | An electrolytic device for decomposition of water has been developed which readily gives hydrogen and oxygen for isotopic measurement with a mass spectrometer. A 20-mul sample can be decomposed quantitatively in 10 min with good reproducibility. The results produced are comparable with those obtained by reduction with uranium. |
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