Synthesis and reactivity of a 5-azido analogue of neuraminic acid |
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Authors: | Matsuoka K Oka H Terunuma D Kuzuhara H |
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Institution: | Department of Functional Materials Science, Faculty of Engineering, Saitama University, Urawa, Japan. koji@fms.saitama-u.ac.jp |
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Abstract: | A peracetylated phenyl 2-thioglycoside (1) of a 5-azido analogue neuraminic acid methyl ester was prepared from a known 5-amino precursor by a diazo transfer reaction. Glycosidation of 1 by alcohols proceeded smoothly in CH3CN to give alpha-sialylated products in good yield. |
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