Solid-state NMR crystallography through paramagnetic restraints |
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| Authors: | Luchinat Claudio Parigi Giacomo Ravera Enrico Rinaldelli Mauro |
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| Affiliation: | Magnetic Resonance Center (CERM), University of Florence, via Sacconi 6, Sesto Fiorentino, Italy. luchinat@cerm.unifi.it |
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| Abstract: | Pseudocontact shifts (PCSs) measured by solid-state NMR spectroscopy (SS-NMR) on microcrystalline powders of a paramagnetic metalloprotein permit NMR crystallography. Along with other restraints for SS-NMR experiments, the protein molecular structure as well as the correct crystal packing are obtained. |
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