| 一类新颖含C60复合材料的合成及其光限制效应的研究 |
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| 引用本文： | 夏海平,朱从善.一类新颖含C60复合材料的合成及其光限制效应的研究[J].光学学报,1997,17(12):634-1637. |
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| 作者姓名： | 夏海平 朱从善 |
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| 作者单位： | 中国科学院上海光学精密机械研究所 |
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| 摘 要： | 报道了在Ｃ６０与ＮＨ２（ＣＨ２）３Ｓｉ（ＯＣ２Ｈ５）３中的胺基反应生成Ｃ６０－ＮＨ２（ＣＨ２）３Ｓｉ（ＯＣ２Ｈ５）３物质后引入ｒ－缩水甘油醚基丙基三甲氧基硅烷「ＣＨ２ＯＣＨＣＨ２ＯＣＨ２ＣＨ２ＣＨ２Ｓｉ（ＯＣＨ３）３，３－Ｇｌｙｃｉｄｏｘｙｐｒｏｐｌｔｒｉｍｅｔｈｏｘｙｓｉｌａｎｅ，简称ＫＨ５６０」与二甲基二乙氧基硅烷「（ＣＨ３）２Ｓｉ（ＯＣ２Ｈ５）２，Ｄｉｅｔｈｏｘｙｄｉｍｅｔｈｙｌｓｉｌａｎｅ
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| 关 键 词： | 复合材料 光限制效应 碳60 富勒烯 |
| 收稿时间： | 1996/12/16 |
Fabrication of Ormosils Connecting with C 60 and Its Optical Limiting Effect |
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| Xia Haiping,Zhu Congshan,Gan Fuxi.Fabrication of Ormosils Connecting with C 60 and Its Optical Limiting Effect[J].Acta Optica Sinica,1997,17(12):634-1637. |
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| Authors: | Xia Haiping Zhu Congshan Gan Fuxi |
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| Abstract: | The sol gel process of C 60 NH 2(CH 2) 3Si(OC 2H 5) 3(C 60 3 Aminopro pyltriethoxysilane or C 60 KH550) mixing with CH 2OCHCH 2O(CH 2) 3Si(OCH 3) 3 (3 Glcidoxypropltrimethoxysilane or KH560) and (CH 3) 2Si(OC 2H 5) 2 (Diethoxy dimethymethylsilane, DTDS) were reported. The ormosils connecting with C 60 possessed good flexibility and mechanical strength. BET experiment showed that these materials have quite small pore. The compound can be polished on the machine. By using a Nd:YAG laser with 10 ns pulse duration and 532 nm wavelength, the optical limiting behavior of C 60 connecting with gel net was measured and demonstrated. |
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| Keywords: | C 60 ormosil optical limiting effect |
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