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Structure of 6,13-bis(N, N-dimethylcarbamoyl) thioquinanthrene
Authors:Andrzej?Ma?lankiewicz  mailto:maslankiewicz@slam.katowice.pl"   title="  maslankiewicz@slam.katowice.pl"   itemprop="  email"   data-track="  click"   data-track-action="  Email author"   data-track-label="  "  >Email author,Ewa?Michalik,Tadeusz?G?owiak,Andrzej?Kowalski
Affiliation:(1) Department of Organic Chemistry, The Medical University of Silesia Jagiello"nacute"ska 4, 41-200, Sosnowiec, Poland;(2) Institute of Chemistry, University of Wroc"lstrok"aw, F.Joliot-Curie 14, 50-383, Wroc"lstrok"aw, Poland;(3) Oxford Diffraction, ul. Rogowska 127A, 54-440, Wroc"lstrok"aw, Poland
Abstract:
The crystal structure of 6,13-bis-(N,N-dimethylcarbamoyl)thioquinanthrene 3 has been determined as monoclinic, with space group P2(1)/c with lattice parameters a = 10.044(2) Å, b = 21.385(4) Å, c = 10.889(3) Å, beta = 102.92(3)°, Z = 4 and Dcalc = 1.342 Mg/m3. The middle 1,4-dithiin ring in the title compound 3, C24H20N4O2S2 is in a boat conformation with the dihedral angle between the planes of the aromatic rings 132.45(8)°.
Keywords:1,4-Dithiin ring  dimethylcarbamoyl group  quinoline derivatives
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